Enhanced comprehensive properties of stereolithography 3D printed alumina ceramic cores with high porosities by a powder gradation design  

作　　者：Xiang Li Haijun Su Dong Dong Di Zhao Yuan Liu Zhonglin Shen Hao Jiang Yinuo Guo Haifang Liu Guangrao Fan Wenchao Yang Taiwen Huang Jun Zhang Lin Liu Hengzhi Fu 

机构地区：[1]State Key Laboratory of Solidification Processing,Northwestern Polytechnical University,Xi’an 710072,China [2]Research and Development Institute of Northwestern Polytechnical University in Shenzhen,Shenzhen 518057,China

出　　处：《Journal of Materials Science & Technology》2022年第36期264-275,共12页材料科学技术（英文版）

基　　金：financially supported by the National Natural Science Foundation of China(Nos.52130204,52174376,51822405);Guangdong Basic and Applied Basic Research Foundation(No.21201910250000848);Science and Technology Innovation Team Plan of Shaan Xi Province(No.2021TD-17);The Youth Innovation Team of Shaanxi Universities;Joint Research Funds of the Department of Science&Technology of Shaanxi Province and NPU(2020GXLH-Z-024);Key R&D Program of Shaan Xi Province(No.2019ZDLGY 04-04);Fundamental Research Funds for the Central Universities(No.D5000210902);Innovation Foundation for Doctor Dissertation of Northwestern Polytechnical University(Nos.CX2021056 and CX2021066),China。

摘　　要：Ceramic cores with complex structures and optimized properties are critical for hollow turbine blades applied in aeroengines.Compared to traditional methods,additive manufacturing(AM)presents great advantages in forming complex ceramic cores,but how to balance the porosity and strength is an enormous challenge.In this work,alumina ceramic cores with high porosity,moderate strength,and low high-temperature deflection were prepared using stereolithography(SLA)3D printing by a novel powder gradation design strategy.The contradiction between porosity and flexural strength is well adjusted when the mass ratio of the coarse,medium,and fine particles is 2:1:1 and the sintering temperature is 1600℃.The fracture mode of coarse particles in sintered SLA 3D printing ceramic transforms from intergranular fracture to transgranular fracture with the increase of sintering temperature and the proportion of fine powders in powder system.The sintered porosity has a greater influence on the high-temperature deflection of SLA 3D printed ceramic cores than grain size.On this basis,a"non-skeleton"microstructure model of SLA 3D printed alumina ceramic cores is created to explain the relationship between the sintering process and properties.As a result,high porosity(36.4%),appropriate strength(50.1 MPa),and low high-temperature deflection(2.27 mm)were achieved by optimizing particle size gradation and sintering process,which provides an insight into the important enhancement of the comprehensive properties of SLA 3D printed ceramic cores.

关 键 词：Ceramic cores Stereolithography(SLA) Powder gradation design Sintering temperature Comprehensive properties 

分 类 号：V261[航空宇航科学与技术—航空宇航制造工程] TQ174.758.11[化学工程—陶瓷工业]