北京市农用地土壤重金属可提取态标准物质研制  

Preparation of Extractable Heavy Metal from Agricultural Soil Reference Materials of Beijing

作　　者：袁建[1] 王亚平[2] 许春雪[2] 安子怡[2] 冯硕 YUAN Jian;WANG Ya-ping;XU Chun-xue(Analytical Laboratory of Beijing Research Institute of Uranium Geology,Beijing 100029;National Research Center for Geoanalysis,Beijing 100037)

机构地区：[1]核工业北京地质研究院,北京100029 [2]国家地质实验测试中心,北京100037

出　　处：《安徽农业科学》2023年第5期194-197,共4页Journal of Anhui Agricultural Sciences

基　　金：科技部专项(121201105000168509)。

摘　　要：为了更好地配合全国农用地土壤污染详查计划,使测试数据质量得到监控,研制了2个北京市农用地土壤重金属有效态标准物质,样品采自北京市通州区永乐店镇德仁务村、平谷区刘家店孔城峪村,样品类型覆盖了北京市农用地土壤的主要类型。经检验表明样品的均匀性和稳定性良好。选择不同系统具有国家级计量认证资质的10家实验室参与定值测试工作,定值参数12项,尽量选用2种以上不同原理的已知准确的可靠的分析方法,按照规范要求对数据进行统计处理和异常值剔除,给出了2个候选物样品的推荐值和不确定度。In order to better coordinate with the national soil pollution survey plan,the quality of test results could be monitored.Two reference materials for extractable heavy metals from agricultural soil in Beijing were developed.Samples were collected from Derenwu Village of Tongzhou District,Kongchengyu Village of Pinggu District.The sample types covered the main types of Beijing agricultural land soil.The test results showed that the homogeneity and stability of the samples were good.The results from 10 laboratories which had the national level measurement authentication qualification were combined to confirm certified values and uncertainty of 12 components.The certified values and uncertainties of two candidate samples were given by using two or more known,accurate and reliable analysis methods with different principles.According to the requirements of the specification,the results were statistically processed and outliers were removed,and the recommended values and uncertainties of two candidate samples were given.

关 键 词：重金属 农用地土壤 可提取态 标准物质 

分 类 号：X53[环境科学与工程—环境工程]