水体中合成麝香检测方法的研究进展  

Research Progress on Detection Methods for Synthetic Musk in Water Body

作　　者：刁子珊 陈卫东 马慧 解晓敏 李赟 张晓寒 DIAO Zishan;CHEN Weidong;MA Hui;XIE Xiaomin;LI Yun;ZHANG Xiaohan(School of Environmental Science and Engineering,Shandong University,Qingdao 266237,China;Centre Testing International Pinbiao(Shanghai)Co.,Ltd.,Shanghai 201100,China;Centre Testing International(Qingdao)Co.,Ltd.,Qingdao 266000,China;Environmental Monitoring Station of Pudong New District,Shanghai 200135,China;College of Resources and Environmental,Qingdao Agricultural University,Qingdao 266109,China)

机构地区：[1]山东大学环境科学与工程学院,青岛266237 [2]上海华测品标检测技术有限公司,上海201100 [3]青岛市华测检测技术有限公司,青岛266000 [4]上海浦东新区环境监测站,上海200135 [5]青岛农业大学资源与环境学院,青岛266109

出　　处：《理化检验（化学分册）》2023年第5期612-620,共9页Physical Testing and Chemical Analysis(Part B:Chemical Analysis)

基　　金：国家自然科学基金(22206110);山东省自然科学基金(ZR2022QB072、ZR2022QD038)。

摘　　要：合成麝香被广泛应用于个人护理产品和生活用品中,在环境中的污染程度呈逐年上升的趋势,准确测定环境中合成麝香的含量具有重要意义。综述了水体中合成麝香的前处理方法(包括固相萃取法、固相微萃取法、液液萃取法、液液微萃取法、索氏提取法、超声辅助提取法、加速溶剂萃取法和QuEChERS等)和仪器分析方法(包括气相色谱-质谱法、气相色谱-串联质谱法、高效液相色谱法、液相色谱-串联质谱法和新型荧光光谱法等),并对相关研究领域的发展趋势进行了展望(引用文献52篇)。Synthetic musk was widely used in personal care products and daily necessities,and the pollution level in the environment was increasing with years.It was of great significance to accurately determine synthetic musk in the environment.The pretreatment methods(including solid phase extraction,solid phase microextraction,liquid-liquid extraction,liquid-liquid micro-extraction,Soxhlet extraction,ultrasound-assisted extraction,accelerated solvent extraction and QuEChERS)and instrumental analysis methods(including gas chromatography-mass spectrometry,gas chromatography-tandem mass spectrometry,high performance liquid chromatography,liquid chromatography-tandem mass spectrometry and new fluorescence spectrophotometry)of synthetic musk in water body were reviewed,and the development trend of relevant research field was prospected(52ref.cited).

关 键 词：合成麝香 水体 前处理方法 仪器分析方法 研究进展 

分 类 号：O65[理学—分析化学]