Development of solid base catalyst X/Y/MgO/-Al_(2)O_(3) for optimization of preparation of biodiesel from Jatropha curcas L.seed oil  

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作  者:Rui WANG Song YANG Shitao YIN Baoan SONG Pinaki SBHADURY Wei XUE Shuwei TAO Zhaohui JIA Da LIU Liang GAO 

机构地区:[1]Center for Research and Development of Fine Chemicals,Key Laboratory of Green Pesticide and Agricultural Bioengineering,Ministry of Education,Guizhou University,Guiyang 550025,China [2]Department of Biology and Environment Engineering,Guiyang College,Guiyang 550005,China

出  处:《Frontiers of Chemical Science and Engineering》2008年第4期468-472,共5页化学科学与工程前沿(英文版)

基  金:supported by the Key Science and Technology Project of Guizhou(No.20076004).

摘  要:The preparation and regeneration conditions of the identified catalyst X/Y/MgO/?-Al2O3 with high catalytic activity were studied and optimized. The biodiesel was prepared by transesterification of Jatropha curcas seed oil produced in Guizhou with methanol at its reflux temoerature in the presence of X/Y/MgO/?-Al2O3 . The pilot plant tests were carried out in a 100 L reaction vessel. Both average yield and fatty acid methyl esters (FAME) content reached more than 96.50% under the optimum reaction conditions of the pilot plant tests designed with an oil/methanol molar ratio of 1 : 10, catalyst concentration of 1.00%, and reaction time of 3 h at reflux temperature. In addition, analysis shows that the quality of biodiesel meets the standard EN 14214.

关 键 词:Solid base catalyst Jatropha curcas oil Transesterification reaction Pilot plant test 

分 类 号:O64[理学—物理化学]

 

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