3-甲基吡啶的合成工艺研究  

Study on the Synthetic Process of 3-Methylpyridine

作　　者：周浩 齐勇 汪娟娟 陈洋 ZHOU Hao;QI Yong;WANG Juan-juan;CHEN Yang(Anhui Ruibang Biotechnology Co.Ltd.,Maanshan 243100,China)

机构地区：[1]安徽瑞邦生物科技有限公司,安徽马鞍山243100

出　　处：《安徽化工》2023年第4期74-76,80,共4页Anhui Chemical Industry

摘　　要：简要介绍了3-甲基吡啶的用途和微波液相的合成方法。实验考查并优化了碳源种类、氨源种类、催化剂用量、不同溶剂、反应时间等一系列条件,最终3-甲基吡啶的选择性和收率分别达到65%和71.2%。The application of 3-methylpyridine and the synthesis method of microwave liquid phase were briefly intro⁃duced.Different carbon sources,ammonia sources,catalyst dosages,different solvents and reaction time were explored.A series of conditions such as carbon source type,ammonia source type,catalyst dosage,different solvents and reaction time were investigated and optimized in the experiment.Finally,the selectivity and yield of 3-methylpyridine reached 65%and 71.2%.

关 键 词：3-甲基吡啶 微波法 碳源 氨源 

分 类 号：TQ253.2[化学工程—有机化工]