高精度陶瓷平板分离膜的制备及性能研究  

Preparation and Performance Study of Ceramic Flat Separation Membranes

作　　者：介志远 赵世凯[1] 张久美[1] 李亮[1] 李洪达 李杰[1] 李小勇[1] 徐传伟[1] 张珂珂 张子豪 JIE Zhi-Yuan;ZHAO Shi-Kai;ZHANG Jiu-Mei;LI Liang;LI Hong-Da;LI Jie;LI Xiao-Yong;XU Chuan-Wei;ZHANG Ke-Ke;ZHANG Zi-Hao(Shandong Industrial Ceramic Research&Degisn insitute Co.Ltd.,Zibo 255000,China)

机构地区：[1]山东工业陶瓷研究设计院有限公司,山东淄博255000

出　　处：《现代技术陶瓷》2023年第5期509-516,共8页Advanced Ceramics

摘　　要：本文以喷涂过渡层的氧化铝板为膜板支撑体,在其上采用动态喷涂法制备分离膜层。通过SEM,孔径分析等手段对所得样品进行表征。探究不同烧成温度,喷涂增重,膜浆固含对陶瓷膜孔径,形貌,膜厚的影响,得出最佳的陶瓷平板膜制备条件。结果表明:当烧成温度为1060℃,氧化铝膜浆固含为35%,焙烧后喷涂增重在0.4%~0.6%之间时,膜厚与膜形貌达到最优。陶瓷平板膜的孔径在90nm左右,水通量在0.3MMH。This article used aluminum oxide plate with a sprayed transition layer as the membrane support,and used dynamic spraying method to prepare a separation membrane layer on it.The obtained samples were characterized by SEM,pore size analysis,and other methods.To explore the influence of different firing temperature,spraying weight increase and solid content of membrane slurry on the pore diameter,morphology and thickness of Ceramic membrane,and to obtain the best preparation conditions of Ceramic flat membrane.The results showed that when the sintering temperature was 1060°C,the solid content of the alumina membrane slurry was 35%,and the spray weight gain after calcination was between 0.4%~0.6%,the film thickness and morphology reached the optimal level.The pore size of the ceramic flat membrane was around 9Onm,and the water flux Was 0.3MMH.

关 键 词：陶瓷平板膜 氧化铝 水通量 

分 类 号：TB332[一般工业技术—材料科学与工程]