交联剂TAIC生产工艺的研究  

Research on the production process of crosslinking agent TAIC

作　　者：张新江 李大庆 ZHANG Xinjiang;LI Daqing(Hangzhou Keli Chemical Co.,Ltd.,Hangzhou 310018,China)

机构地区：[1]杭州科利化工股份有限公司,浙江杭州310018

出　　处：《氯碱工业》2024年第1期35-38,共4页Chlor-Alkali Industry

摘　　要：通过对试验获得的TAIC产品气相含量、液相含量、色度和酸值4个控制指标进行对比分析,确定了收率为90%的最佳原料配比及反应条件。原料的质量比为:m(异氰尿酸三钠):m(氯丙烯):m(催化剂):m(脱水剂):m(溶剂)=100:130:2.4:1:300;反应温度控制在95℃。By comparing and analyzing the four control indicators of gas phase content,liquid phase content,chromaticity,and acid value of TAIC products obtained from experiments,the optimal raw material ratio and reaction conditions with a yield of over 90%were determined.The mass ratio of raw materials was m(trisodium isocyanurate):m(allyl chloride):m(catalyzer):m(dehydrating agent):m(solvent)=100:130:2.4:1:300.The reaction temperature was controlled at 95℃.

关 键 词：三烯丙基异氰脲酸酯 异氰尿酸三钠 氯丙烯 反应温度 原料配比 色度 酸值 收率 

分 类 号：TQ314.269[化学工程—高聚物工业]