磷虾油中有机砷脱除工艺优化  

Removal Process Optimization of Organic Arsenic from Krill Oil

作　　者：方素琼 朱东奇 林锦淮 杨继国 FANG Suqiong;ZHU Dongqi;LIN Jinhuai;YANG Jiguo(Sirio Pharma Co.,Ltd.,Shantou 515041,Guangdong,China;South China Institute of Collaborative Innovation,Dongguan 523808,Guangdong,China;College of Food Sciences and Engineering,South China University of Technology,Guangzhou 510640,Guangdong,China;Heyuan Branch,Guangdong Laboratory for Lingnan Modern Agriculture,Heyuan,517000,Guangdong,China)

机构地区：[1]仙乐健康科技股份有限公司,广东汕头515041 [2]华南协同创新研究院,广东东莞523808 [3]华南理工大学食品科学与工程学院,广东广州510640 [4]岭南现代农业科学与技术广东省实验室河源分中心,广东河源517000

出　　处：《食品研究与开发》2024年第9期111-117,共7页Food Research and Development

基　　金：广东省重点领域研发计划项目(2022B0202010001);岭南现代农业科学与技术广东省实验室河源分中心自主科研项目(DT20220004);河源市科技计划项目(河科平台2022大专项010)。

摘　　要：选用椰壳活性炭和水为脱除剂,对磷虾油中有机砷进行脱除。以有机砷的脱砷率为指标,考察脱砷温度、椰壳活性炭添加量、水添加量、脱砷时间4个因素对磷虾油中有机砷脱除的影响,采用Box-Behnken设计响应面试验优化磷虾油有机砷脱除工艺,并考察脱除前后磷虾油主要质量指标。结果表明:椰壳活性炭添加量10.0%,水添加量39.0%、脱砷时间5.5 h时,磷虾油中有机砷可以由初始的4.10 mg/kg降低至1.28 mg/kg,脱砷率为68.68%,脱除前后,磷虾油中磷脂、虾青素含量、酸价、过氧化值等主要指标没有明显变化。In this paper,with coconut shell⁃activated carbon and water as removal agents,organic arsenic in krill oil was removed.Taking the arsenic removal rate of organic arsenic as an index,the effects of arsenic re⁃moval temperature,the addition of coconut shell⁃activated carbon,water addition and arsenic removal time on the removal of organic arsenic were investigated.The removal process was optimized by Box⁃Behnken design,and the main quality indexes of krill oil before and after removal were analyzed.The results showed the addi⁃tion of coconut shell⁃activated carbon 10.0%of krill oil′s mass,water addition 39.0%of krill oil′s mass,and arsenic removal time 5.5 h.The organic arsenic was reduced from the initial 4.10 mg/kg to 1.28 mg/kg,with the removal rate of 68.68%.Before and after removal,phospholipids,astaxanthin,acid value and peroxide value in krill oil did not change significantly.

关 键 词：磷虾油 有机砷 椰壳活性炭 工艺优化 脱砷率 

分 类 号：TS225.24[轻工技术与工程—粮食、油脂及植物蛋白工程]