油田污水过滤罐活性炭原位氧化再生  

In situ oxidation and regeneration of activated carbon in oilfield sewage tanks

作　　者：朱博[1] 南晓佳 杨玲 王春勇 李金玉 吕雪 郑佳乐 ZHU Bo;NAN Xiao;YANG Ling;WANG Chunyong;LI Jinyu;LU Xue;ZHENG Jiale(School of Chemical and Environmental Engineering,Liaoning University of Technology,Jinzhou 121001,China;Panjin Dober Environmental Technology Inc,Panjin 124000,China)

机构地区：[1]辽宁工业大学化学与环境工程学院,辽宁锦州121001 [2]盘锦道博尔环保科技股份有限公司,辽宁盘锦124000

出　　处：《应用化工》2024年第6期1310-1314,共5页Applied Chemical Industry

基　　金：辽宁省博士启动基金(2021-BS-256);2023年省级大学生创新创业训练计划(S202310154028)。

摘　　要：采用过硫酸铵(APS)热活化复合超声波及甲醇萃取的方法原位再生油田污水过滤罐活性炭,考察了初始pH值、过硫酸铵用量、反应温度、反应时间、超声波强化APS功率及甲醇浓度对活性炭再生效果的影响。结果表明,APS热活化复合超声波及甲醇萃取的方法再生效果更好。当初始pH值为7,APS溶液浓度为500 g/L,反应温度为70℃,反应时间为30 min,超声强度为60%,甲醇萃取浓度100%,再生2次,活性炭的再生效率分别为79.16%和66.84%。The activated carbon from oilfield wastewater filter tank was regenerated in situ by ammonium persulfate(APS)thermal activation combined with ultrasonic and methanol extraction.The effect of the initial pH value,the dose of ammonium peroxide,the reaction temperature,the reaction time,the ultrasonic enhanced APS power and the methanol concentration on the adsorption efficiency of the regenerated activated carbon was investigated.The results show that the combination of APS thermal activation with ultrasound and methanol extraction results in better regeneration.When the initial pH value was 7,the APS solution concentration was 500 g/L,the reaction temperature was 70℃,the reaction time was 30 min,the ultrasonic intensity was 60%,the methanol extraction concentration was 100%,and the regeneration efficiency of activated carbon was 79.16%and 66.84%,respectively.

关 键 词：过硫酸盐 活性炭 油田污水 超声波 

分 类 号：TQ118[化学工程—无机化工] TE991[石油与天然气工程—石油机械设备]