氮苯基丙二硫酯化合物的合成与表征  

Synthesis and Characterization of Azaphenyl Propylene Disulfide Compound

作　　者：马书修 崔晁瑜 甘贞洁 刘文博 MA Shu-xiu;CUI Chao-yu;GAN Zhen-jie;LIU Wen-bo(School of Chemical and Printing-Dyeing Engineering,Henan University of Engineering,Henan Zhengzhou 451191,China)

机构地区：[1]河南工程学院化工与印染工程学院,河南郑州451191

出　　处：《广州化工》2024年第15期166-167,172,共3页GuangZhou Chemical Industry

基　　金：2022年河南省高等学校大学生创新训练计划项目(No:202211517001);河南省青年科学基金项目(No:242300421614);2021年河南工程学院博士培育基金项目(No:D2021013)。

摘　　要：详细介绍了一种探究性的有机化学综合实验的设计,一种氮苯基丙二硫酯化合物的设计合成与表征。实验利用苯胺,甲醛水溶液与硫代乙酸为原料,在乙醇溶液中,通过“一锅法”得到氮苯基丙二硫酯化合物,并对产物结构进行简要的分析归纳。本实验主要针对化学化工专业类学生在有机化学实验中理论联系实践不足的问题,让学生从探究性的有机化学实验中提高分析与总结的综合能力。The synthesis of an exploratory organic chemistry synthesis experiment was introduced,and a azaphenyl propylene disulfide compound was synthesized and characterized in detail.In this experiment,aniline,formaldehyde aqueous solution and thioacetic acid were used as reagents.In ethanol solution,the azaphenyl propylene disulfide compound were obtained by “one-pot” method,and the structure of the product was briefly analyzed and summarized.This experiment mainly aimed at the problem of insufficient connection between theory and practice in the exploratory experiment of Organic Chemistry for students majoring in Chemistry and Chemical Engineering,and enabled students to improve their comprehensive ability of analysis and summary from exploratory Organic Chemistry experiments.

关 键 词：苯胺 硫代乙酸 氮苯基丙二硫酯 硫酯化合物 

分 类 号：G642[文化科学—高等教育学]