乙二醇-水体系纳米银的制备及其抗菌性能  

Preparation and antibacterial properties of silver nanoparticles synthesized in glycol-water solvents

作　　者：范璐璐 陈延明[1] 王立岩[1] 张智慧 Fan Lulu;Chen Yanming;Wang Liyan;Zhang Zhihui(School of Petrochemical Engineering,Shenyang University of Technology,Shenyang 111003)

机构地区：[1]沈阳工业大学石油化工学院,辽阳111003

出　　处：《化工新型材料》2024年第S02期265-271,共7页New Chemical Materials

摘　　要：采用溶液化学法,以油酸钠为表面活性剂,硝酸银水溶液为前驱体,乙二醇为还原剂和溶剂,通过调控温度和水的加入量,在乙二醇-水体系中制备了一系列不同尺寸的球形银纳米颗粒(AgNPs)。通过紫外-可见光(UV-Vis)光谱、X射线衍射(XRD)、透射电镜(TEM)和高清透射电镜(HRTEM)对AgNPs的光学性质和晶体结构进行了详细表征。采用平板浇注法测定了不同尺寸AgNPs的抗菌活性。结果表明:通过调控反应温度和乙二醇/水体积比,可在温和条件下制备出不同尺寸的AgNPs。AgNPs对金黄色葡萄球菌和大肠杆菌均具有显著的抑菌效果。A series of spherical silver nanoparticles(AgNPs)of different sizes were prepared in ethylene glycol-water solvent by solution chemistry using sodium oleate as surfactant,silver nitrate aqueous solution as precursor,ethylene glycol as reducing agent and solvent by adjusting the temperature and the amount of water added.The optical properties and crystal structure of AgNPs were thoroughly characterized by UV-Vis spectroscopy,XRD diffraction,TEM and HRTEM.The antibacterial activity of AgNPs of different sizes was determined by plate casting method.The results showed that AgNPs of different sizes could be prepared under mild conditions by adjusting reaction temperature and ethylene glycol/water volume ratio.AgNPs had significant antibacterial effect against Staphylococcus aureus and Escherichia coli.

关 键 词：AGNPS 溶液化学法 抗菌性能 平板浇注法 

分 类 号：TB383[一般工业技术—材料科学与工程]