活性炭负载N掺杂TiO_(2)的制备与光催化性能研究  

Preparation and Photocatalytic Activity of N-doped TiO_(2)Loaded on Activated Carbon

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作  者:邵文博 田文杰 林晓霞[1] SHAO Wen-bo;TIAN Wen-jie;LIN Xiao-xia(School of Materials Engineering,Jingling Institute of Technology,Nanjing 211169,China)

机构地区:[1]金陵科技学院材料工程学院,江苏南京211169

出  处:《安徽化工》2024年第5期55-57,共3页Anhui Chemical Industry

基  金:江苏省大学生创新训练计划(202313573107Y);江苏省高校哲学项目(2020SJA0545)。

摘  要:采用一步溶胶-凝胶法制备活性炭负载N掺杂TiO_(2)(N-TiO_(2)/AC)复合物。利用X射线衍射(XRD)、扫描电子显微镜(SEM)等对样品进行晶型和形貌表征。XRD结果表明,所制备样品具有锐钛矿晶型结构;SEM照片显示,所制备N-TiO_(2)粒子均匀地分散在活性炭上。通过在可见光照下降解染料甲基橙(MO),评价N-TiO_(2)/AC的光催化性能。结果表明,与N-TiO_(2)相比,N-TiO_(2)/AC对甲基橙的降解率提升了21.5%;经6次循环使用后,N-TiO_(2)/AC的催化降解率仍高于82%。N-doped TiO_(2)supported on activated carbon(N-TiO_(2)/AC)was prepared by one step sol-gel method.The prepared samples were characterized by X-ray diffraction(XRD)and scanning electron microscopy(SEM).XRD indicates that the prepared samples had anatase crystal structure.SEM indicates that the prepared TiO_(2)particles were uniformly dispersed on the activated carbon.The photocatalytic performance of N-TiO_(2)/AC was evaluated,by degrading dye methyl orange(MO)under visible light irradiation.The results showed N-TiO_(2)/AC increased the degradation rate of methyl orange by 21.5%compared with N-TiO_(2),the photocatalytic rate of N-TiO_(2)/AC was sill higher than 82%after 6 cycles of use.

关 键 词:活性炭 负载 N掺杂TiO_(2) 光催化 

分 类 号:O643[理学—物理化学]

 

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