物理化学综合实验设计——双金属磷化物的制备及应用  

Comprehensive Experiment Design of Physical Chemistry——Preparation and Application of Bimetal Phosphides

作　　者：宋琪 李璟明 努尔古丽·拉提莆 明惠 范士广 吴梅 侯军伟 SONG Qi;LI Jingming;Nurgul·LATEP;MING Hui;FAN Shiguang;WU Mei;HOU Junwei(China University of Petroleum-Beijing At Karamay,Chemistry&Chemical Engineering Experimental Teaching Demonstration Center of Autonomous Region,Karamay 834000,China)

机构地区：[1]中国石油大学(北京)克拉玛依校区,化学与化工自治区级实验教学示范中心,新疆克拉玛依834000

出　　处：《化工管理》2024年第34期52-56,共5页Chemical Management

基　　金：“中国石油大学(北京)克拉玛依校区2023年教育教学研究项目”(JG2023026)的研究成果;“新疆维吾尔自治区基本科研业务费”(XJEDU2023P169);“克拉玛依市创新人才专项”(20222023hjcxrc0011)资助。

摘　　要：文章设计了一个双金属磷化物的制备及电催化水分解产氢物理化学综合实验。通过电沉积、化学气相沉积法制备了双金属磷化物催化剂,在三电极体系中测试其电催化析氢性能,并通过SEM对其形貌进行表征。将科研工作的前沿热点引入实验教学当中,加深了学生对催化剂制备、电化学性能测试和表征的认识,提升学生的科学素养和综合实验技能,为培养高素质应用型工程技术人才打下基础。A comprehensive experiment on the preparation of bimetal phosphides and the physical chemistry of hydrogen production by electrocatalytic water decomposition was designed.The bimetal phosphides were prepared by electrodeposition and chemical vapor deposition,and the electrocatalytic hydrogen evolution performance was tested in a three-electrode system,and the morphology was characterized by SEM.By introducing the frontier of scientific research into experimental teaching,students’understanding of catalyst preparation,electrochemical performance testing and characterization could be deepened,students’scientific literacy and comprehensive experimental skills could be improved,and a foundation would be laid for cultivating highquality applied engineering and technical talents.

关 键 词：物理化学 综合实验 电催化 析氢反应 

分 类 号：G642.0[文化科学—高等教育学]