油田水中F^-,Cl^-,Br^-,NO_2^-,SO_4^(2-)的离子色谱分析  被引量:18

Determination of Total Fluoride,Chloride,Bromid,Nitrite, Sulfate in the Oil Field Water by Ion Chromatograph

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作  者:郭庭秀[1] 

机构地区:[1]中国石化河南油田分公司石油勘探开发研究院,南阳473132

出  处:《现代科学仪器》2002年第6期12-13,共2页Modern Scientific Instruments

摘  要:采用离子色谱法测定油田水中的氟、氯、溴、亚硝酸根和硫酸根的含量。以碳酸钠为流动相 ,用IonPacAS9 HC分析柱分离 ,分离效果理想 ,灵敏度较高。F-,Cl-,Br-,NO-2 和SO2 -4的检测限分别为 0 .0 1mg/L ,0 .0 2mg/L ,0 .0 3mg/L ,0 .0 1mg/L ,0 .0 2mg/L ,具有良好的线性和重现性。对油田水样品进行测定 ,其结果与化学法分析结果对比 。An ion chromatograph system for the determination of F -,Cl -,Br -,NO - 2,SO 2- 4 in oil field water was described. The mobile phase was sodium carbonate. The analytical column was IonPac AS9 HC. The detection limits of general anions were F -0.01mg/L, Cl -0.02mg/L, Br -0.03mg/L, NO - 20.01mg/L, SO 2- 40.02mg/L., respectively. Experiment results showed that linear relationship and repeatability were good. This method was used to determine general anions in oil field water, and the result coincided with the chemical analytical method very well. The method was simple, rapid, reliable and inexpensive.

关 键 词:油田水 离子色谱    亚硝酸根 硫酸根 

分 类 号:O657.7[理学—分析化学]

 

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