生鲜乳与乳品加工产品中高氯酸盐污染现状及检测方法研究进展  

Research Progress of Perchlorate Contamination and Its Detection Methods in Fresh Milk and Dairy Products

作　　者：张强 ZHANG Qiang(Suining Bureau of Agriculture and Rural Affairs,Suining 629000;Suining Agricultural Products Inspection and Monitoring Center,Suining 629000)

机构地区：[1]四川遂宁市农业农村局,遂宁629000 [2]四川遂宁市农产品检验监测中心,遂宁629000

出　　处：《中国奶牛》2025年第1期47-52,共6页China Dairy Cattle

摘　　要：综述了生鲜乳与乳类加工产品中高氯酸盐暴露现状和途径,以及检测方法研究进展。现阶段,国内外鲜乳与乳品加工产品中普遍检出高氯酸盐,养殖环节是高氯酸盐暴露的主要途径。离子色谱法、离子色谱质谱法、液相色谱串联质谱法是高氯酸盐测定的主要方法。其中,离子色谱法操作灵活性高、设备简单,但抗干扰能力较差,目前研究相对较少;离子色谱质谱法能够有效解决高氯酸盐在液相上保留差、稳定性低等问题,获得不错的效果,但该设备成本较高,能检项目较少,限制了方法的推广使用;液相色谱串联质谱法具有使用范围广、成熟可靠、抗干扰能力强等特点,成为研究最多的方法。将来开发符合新质生产力发展要求和新发展理念的鲜乳与乳类加工产品中的高氯酸盐前处理技术,将会是实验室内液相色谱串联质谱法的研究重点。In this paper,perchlorate exposure in fresh milk and processed dairy products was reviewed,as well as the research progress of detection methods.At present,perchlorate is generally detected in fresh milk and dairy products,and culture is the main way of perchlorate explosion.Ion chromatography,ion chromatography mass spectrometry and liquid chromatography mass spectrometry are the main methods for the determination of perchlorate.Among them,ion chromatography has high flexibility,but its anti-interference ability is poor,so there are few researches at present.Ion chromatography mass spectrometry can effectively solve the problems of poor perchlorate retention and low stability in the liquid phase,and obtain good results.However,the high cost of the equipment and few detection items limit the use of the method.Liquid chromatography mass spectrometry has the characteristics of wide application,mature and reliable performance,strong anti-interference ability,and has become the most useful method.In the future,with the development of perchlorate pretreatment technology in fresh milk and dairy products,the development requirements of new quality productivity and new development concepts will be the focus of liquid chromatography mass spectrometry in the laboratory.

关 键 词：高氯酸盐 生鲜乳与乳类加工产品 检测方法 液相色谱串联质谱法 

分 类 号：S823.4[农业科学—畜牧学]