电感耦合等离子体发射光谱与质谱分析技术和应用研究进展  

Progress in Analysis Technology and Application of ICP-OES and ICP-MS

作　　者：冯先进 郑国经[2] FENG Xianjin;ZHENG Guojing(BGRIMM MTC Technology Co.,Ltd.,Beijing 102628,China;Beijing Shougang Iron and Steel Research Institute,Beijing 100085,China)

机构地区：[1]北矿检测技术股份有限公司,北京102628 [2]北京首钢冶金研究院,北京100085

出　　处：《中国无机分析化学》2025年第3期353-362,共10页Chinese Journal of Inorganic Analytical Chemistry

基　　金：国家重点研发计划项目(2021YFC2903105)。

摘　　要：电感耦合等离子体发射光谱(ICP-OES)和电感耦合等离子体质谱(ICP-MS)分析技术都是以ICP为激发源或离子源的无机元素分析技术,在仪器操作、标准物质的配制及进样方式上均有相似之处,成为无机元素测定的得力工具,其溶液进样方式具有朔源性而被各个领域的标准分析方法所采纳,ICP-OES/MS分析方法在标准化方面得到了较快发展。对近年来ICP-OES仪器的现状、分析功能的发展及其应用上的进展进行综述,对ICP-MS分析技术的发展、四极杆电感耦合等离子体质谱分析(ICP-QMS)仪器的进展以及在纳米颗粒分析、生物化学、形态分析、地质年代学等领域中应用的进展进行评述。ICP-OES/MS作为无机元素分析强有力的实用工具,必将在材料研制、工业检测、食品安全、环境监测、医疗卫生防控、石油化工、新能源等行业中,成为无机元素分析测定的主要手段。Inductively coupled plasma optical emission spectrometry( ICP-OES) and inductively coupled plasma mass spectrometry( ICP-MS) are both inorganic element analysis techniques with ICP as the excitation source or ion source.They have similarities in instrument operation,preparation of standard solution and injection method,and are powerful tools for the determination of inorganic elements.The solution injection method is adopted by the standard analysis methods in various fields,and the ICP-OES and ICP-MS analysis methods have been rapidly developed in the standardization aspect.The current status of ICP-OES instruments,the development of analytical functions and the progress in their application were described.The development of ICP-MS analysis technology,the progress of quadrupole inductively coupled plasma mass spectrometry( ICP-QMS) instrument,and the application of nanoparticle analysis,biochemistry,morphological analysis,geochronology and other fields,etc.,were reviewed.As a powerful practical tool for inorganic element analysis,ICP-OES/MS will surely become the main means for the analysis and determination of inorganic elements in materials development,industrial testing,food safety,environmental monitoring,medical and health prevention and control,petrochemical industry,new energy and other industries.

关 键 词：电感耦合等离子体发射光谱 电感耦合等离子体质谱 微型化 智能化 串联四极杆质谱 

分 类 号：O657.31[理学—分析化学] O657.63[理学—化学]