高效液相色谱法测定稳定性尿素增效剂的含量  

Determination of stable urea synergist content by high performance liquid chromatography

作　　者：苗凤媛 李柏松 赵艳慧 MIAO Fengyuan;LI Baisong;ZHAO Yanhui(CN00C Huahe Coal Chemical Co.,Ltd.,Hegang 154100,Heilongjiang Province)

机构地区：[1]中海石油华鹤煤化有限公司,黑龙江鹤岗154100

出　　处：《氮肥技术》2025年第1期32-33,48,共3页Nitrogenous Fertilizer Technology

摘　　要：高效液相色谱法是测定稳定性增值尿素中增效剂含量的分析方法,该方法采用高效液相色谱,220nm波长,1.0mL/min流速,采用C18色谱柱,在室温条件下,对稳定性增值尿素样品进行测定。测定结果的相对标准偏差为0.19%~0.27%(n=4),样品加标回收率为95.6%~102.2%。与分光光度法相比,此方法更简便,分析时间更短,工作效率更高。High performance liquid chromatography is an analytical method for determining the content of synergist in stable value-added urea.This method uses high performance liquid chromatography,220nm wavelength,1.OmL/min flow rate,C18 chromatographic column,and measures the stable value-added urea sample at room temperature.The relative standard deviation of the measurement results is 0.19%~0.27%(n=4),and the recovery rate of sample spiked is 95.6%~102.2%.Compared with spectrophotometry,this method is simpler,has shorter analysis time,and higher work efficiency.

关 键 词：高效液相色谱法 分光光度法 尿素增效剂 测定 效果 

分 类 号：O65[理学—分析化学]