One-pot Synthesis of 1-Aryloxyacety l-4-(4'-nitrophenyloxyacetyl)-thiosemicarbazides under Phase Transfer Catalysis and Microwave Irradiation  

作　　者：Zheng LI Xi Cun WANG 

机构地区：[1]College of Chemistry and Chemical Engineering,Northwest Normal University,Lanzhou 730070

出　　处：《Chinese Chemical Letters》2002年第8期717-720,共4页中国化学快报(英文版)

基　　金：Technological Innovation Engineering of Northwest Normal University (NWNU-KJCXGC-218); Natural Science Foundation of Gansu Province and Youth Foundation of Northwest Normal University.

摘　　要：The 1-aryloxyacetyl-4-(4-nitrophenyloxyacetyl)-thiosemicarbazides (3a-h) are synthe- sized via reaction of 4-nitrophenyloxyacetyl chloride with ammonium thiocyanate and aryloxyacetic hydrazides (2a-h) under phase transfer catalysis and microwave irradiation in excellent yield.The 1-aryloxyacetyl-4-(4-nitrophenyloxyacetyl)-thiosemicarbazides (3a-h) are synthe- sized via reaction of 4-nitrophenyloxyacetyl chloride with ammonium thiocyanate and aryloxyacetic hydrazides (2a-h) under phase transfer catalysis and microwave irradiation in excellent yield.

关 键 词：Diaryloxyacetyl thiosemicarbazide phase transfer catalysis microwave irradiation. 

分 类 号：O625[理学—有机化学]