氯化石蜡-52光引发氯化工艺条件的研究  

Studies of photoinitiation chlorination technique of chlorinated paraffin-52

作　　者：杨智慧[1] 詹晓力[2] 易玲敏[2] 陈丰秋[2] 

机构地区：[1]上海氯碱化工股份有限公司电化厂,上海200241 [2]浙江大学材料与化工学院联合化学反应工程研究所,浙江杭州320027

出　　处：《氯碱工业》2003年第1期37-39,共3页Chlor-Alkali Industry

摘　　要：建立了1套光引发氯化制备氯化石蜡-52的小试实验装置及对反应过程进行分析测试的方法。运用正交设计实验方法,系统地考察了各工艺条件如光强度、光引发时间、氯气流量、反应温度对氯化反应的影响,确定了较佳的工艺参数,为开发万吨级连续化生产装置提供了依据。A small-scale experimental device for preparing chlorinated paraffin-52 by photoinitiation is established,as well as the measurement and test methods of the process.The influence of various process conditions on chlorination are investigated systematically by using the orthogonal-design-experiment method,such as light strength,photoinitiation time,chlorine flow,reaction temperature,etc.The better technical parameters are found out,and the foundation data have been provided for developing the continuous production unit of 10 kt/a.

关 键 词：氯化石蜡-52 光引发 氯化 工艺条件 研究 

分 类 号：TQ03[化学工程]