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作 者:夏维东[1] 王大志[2] 张庶元[3] 万树德[4] 孟祥东[2] 汪海[4]
机构地区:[1]中国科学技术大学热科学与能源工程系,合肥230026 [2]中国科学技术大学材料科学与工程系,合肥230026 [3]中国科学技术大学理化科学中心,合肥230026 [4]中国科学技术大学近代物理系,合肥230026
出 处:《Chinese Journal of Chemical Physics》2003年第1期1-2,共2页化学物理学报(英文)
摘 要:In the product of carbon made from tar oil by plasma pyrogenation, some nanowires, whose diameter is 9~20 nm and whose length is 300 nm were found. The result of X ray Energy Dispersed Spectrum (EDS) indicated that it is a new compound K 2Ti 8O 15 , which has never been reported before. Compared with the corresponding stoichiometry compound K 2Ti 8O 15 , it is a non stoichiometry compound in which two oxygen atoms are absent. It is due to the fact that the intensive deoxidization occured in the experimental process and the valence of titalium is alterable. Its microstructure in detail by high revolution electromicroscopy (HREM) and X ray diffraction were studied.In the product of carbon made from tar oil by plasma pyrogenation, some nanowires, whose diameter is 9 similar to 20 nm and whose length is 300 nm were found. The result of X-ray Energy Dispersed Spectrum (EDS) indicated that it is a new compound K2Ti8O15, which has never been reported before. Compared with the corresponding stoichiometry compound K2Ti8O15, it is a non-stoichiometry compound in which two oxygen atoms are absent. It is due to the fact that the intensive deoxidization occured in the experimental process and the valence of titalium is alterable. Its microstructure in detail by high revolution electromicroscopy (HREM) and X-ray diffraction were studied.
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