微波法固相合成二茂铁基α、β-不饱和酮  

Microwave-assisted synthesis of ferrocenyl α,β-unsaturated ketones in solid phase

作　　者：陆军[1] 陈维一[1] 

机构地区：[1]苏州大学化学化工系,江苏苏州215006

出　　处：《化学研究与应用》2003年第2期265-266,F003,共3页Chemical Research and Application

摘　　要：Microwave irradiation can accelerate the rate of the synthesis reaction of ferrocenyl α,β unsaturated ketones by using KF Al 2O 3 as a catalyst. Six fitled compounds were prepared with microware assisted synthesis. Their structures were characterized by 1H NMR, IR, and elemental analysis.Microwave irradiation can accelerate the rate of the synthesis reaction of ferrocenyl α,β unsaturated ketones by using KF Al 2O 3 as a catalyst. Six fitled compounds were prepared with microware assisted synthesis. Their structures were characterized by 1H NMR, IR, and elemental analysis.

关 键 词：微波法 固相合成 二茂铁基α β-不饱和酮 氧化铝 氟化钾 固体碱催化剂 

分 类 号：O627.81[理学—有机化学] O621.392[理学—化学]