N-马来酰基-氨基丙酸丁酯微乳液的微波聚合  

Study on microwave radiation polymerization of N-maleoyl- alanine butyl ester microemulsion

作　　者：黄梅芳[1] 刘朋生[1] 

机构地区：[1]湘潭大学化学学院,湖南湘潭411105

出　　处：《弹性体》2003年第1期6-8,共3页China Elastomerics

基　　金：湖南省自然科学基金项目 (0 1JJY30 11)

摘　　要：在微波条件下 ,以十二烷基硫酸钠为乳化剂 ,过硫酸钾为引发剂的N -马来酰基 -氨基丙酸丁酯 (BAM)微乳液聚合。研究了聚合时间对聚合速率和转化率的影响。并用PERKIN -ELMERFTIR - 1710红外光谱仪、PE - 2 40 0有机元素分析仪、DT - 40差热分析仪对聚合物进行了检测。In this paper, polymerization of N-maleoyl-alanine butyl ester (BAM) was studied by means of microwave radiation, using sodium dodecyl sulfate(SDS) as emulsifier and potassium persulfate (KPS)as the initiator, the microemulsion containing N-maleoyl-alanine butyl ester was firstly prepared. Polymerization can be controlled in low temperature by controlling time and power of radiation. The effects of microwave radiation time was investigated. At the same time, the polymer was characterized by IR, TG and elemental analysis as well.

关 键 词：N-马亚酰基-氨基丙酸丁酯 微乳液 微波聚合 热性能 

分 类 号：TQ323.9[化学工程—合成树脂塑料工业]