柱色谱分离提纯蔗糖-6-乙酸酯  

Purifying Sucrose-6-Acetate by Column Chromatography

作　　者：张英[1] 粟晖[1] 韦异[1] 廖敬阳[1] 郭霖[1] 

机构地区：[1]广西工学院轻工化工系

出　　处：《食品与发酵工业》2003年第6期60-62,共3页Food and Fermentation Industries

基　　金：广西自治区科技厅自然科学基金资助项目(No .桂科自 0 0 660 0 1);广西工学院科学研究基金资助项目(No .0 0 2 19)

摘　　要：采用薄层色谱法定性 ,以柱色谱法分离提纯蔗糖 6 乙酸酯。蔗糖 6 乙酸酯的平均回收率为 95 0 6 % ,相对标准偏差为 1 0 5 %。并用红外光谱、质谱、核磁共振等方法对蔗糖 6Sucrose 6 acetate was purified by column chromatograph and determined by thin layer chromatograph The average recovery of the method was 95 06% and the relative standard deviations was 1 05% The structure of sucrose 6 acetate was also identified by the methods of IR, MS, NMR

关 键 词：薄层色谱法 柱色谱法 分离提纯 蔗糖—6—乙酸酯 结构鉴定 红外光谱 核磁共振 质谱 

分 类 号：O657.7[理学—分析化学]