2-巯基-1,3,4-噻二唑的合成  

Synthesis of 2-Mercapto-1,3,4-Thiadiazole

作　　者：吕瑞敏[1] 李坤[1] 张雪峰[1] 孟宪兴 田达[1] 

机构地区：[1]山东省化工研究院,山东济南250014

出　　处：《山东化工》2003年第3期9-10,共2页Shandong Chemical Industry

摘　　要：研究了 2 -巯基 -1,3 ,4-噻二唑的合成 ,探讨了反应温度、配料比对产品收率的影响。鉴定了产品的结构 ,测定了产品的熔点及含量 ,其结果与文献值相符。Synthesis of 2-mercapto-1,3,4-thiadiazole was studied,and the optimal reaction conditions were found by experiments.The construction of the product was analyzed by IR and NMR spectrum.Assay and melting point of the product were determinated by analysis,the results accord with theoretical value.

关 键 词：2-巯基-1 3 4-噻二唑 水合肼 二硫化碳 原甲酸三乙酯 红外光谱 核磁振动光谱 

分 类 号：TQ252.5[化学工程—有机化工]