微波辐射下苯并噁唑基吡啶的合成  

Synthesis of Benzoxazolyl-substituted Pyridine Under Microwave Irradiation

作　　者：周红军[1] 王立格[1] 尹帮少[1] 

机构地区：[1]广西师范大学化学化工学院,广西桂林541004

出　　处：《化学研究》2003年第4期39-41,共3页Chemical Research

摘　　要：在微波辐射条件下,利用邻氨基酚和吡啶羧酸在多聚磷酸中的缩合反应,合成了2种苯并唑基取代吡啶 最佳反应条件为:450W辐射4min 相比于常规反应。Under microwave irradiation, two benzoxazolyl-substituted pyridine were synthesized by condensation of o-aminophenol and pyridine carboxylic acid catalyzed by polyphosphoric acid.The optimum reaction condition is as follows: microwave power 450 W and microwave irradiation time 4 min. Compared with the conventional reaction,the reaction time was shortened obviously and the yield was satisfactory.

关 键 词：微波辐射 苯并噁唑基吡啶 合成 催化剂 邻氨基酚 吡啶羧酸 反应条件 杂环化合物 

分 类 号：O626[理学—有机化学]