甲基二甲氧基硅烷的合成  

THE PREPARATION OF METHYLDIMETHOXYSILANE

作　　者：余淑娴[1] 邓仲明[1] 曾纪术[1] 彭勇[1] 李小林[1] 陈其阳 廖洪流 范宏芳 胡音莉 

机构地区：[1]南昌大学化材学院,江西南昌330047 [2]星火化工厂星辰实验室,江西永修330319

出　　处：《南昌大学学报（理科版）》2003年第3期263-266,共4页Journal of Nanchang University(Natural Science)

摘　　要：介绍了由CH3SiHCl2和CH3OH进行酯化反应,采用混合溶剂法制备甲基二甲氧基硅[CH3(OCH3)2SiH],研究了不同溶剂和反应条件对醇解反应的影响,对反应产物进行GC—MS,IR定性定量分析,同时确定了较优的合成条件。Methyldimethoxysilane was synthesized by the esterification reaction of Methyldichlorosilane and Methanol in mixed inert solvents. The effects of different solvents and reaction conditions on the alcoholysis were studied. The composition of products were examined by IR and GC-MS method. And the appropriate reaction conditions were established.

关 键 词：甲基二甲氧基硅烷 合成 甲基二氯硅烷 甲醇 酯化反应 混合溶剂法 

分 类 号：O627.411[理学—有机化学]