样板晶生长法制备Y-TZP/板状氧化铝复相陶瓷的力学性能和可靠性  

MECHANICAL PROPERTIES AND RELIABILITY OF Y-TZP/ PLATELET-ALUMINA COMPOSITES BY TEMPLATED GRAIN GROWTH

作　　者：周振君[1] 杨正方[1] 肖志国 罗昔贤 金雷 

机构地区：[1]天津大学先进陶瓷与加工技术教育部重点实验室,天津300072 [2]大连路明发光科技股份有限公司,大连116025

出　　处：《复合材料学报》2004年第1期28-32,共5页Acta Materiae Compositae Sinica

基　　金：国家高技术研究发展计划(863计划)项目(2002AA324060);中国博士后基金项目(2003033139)

摘　　要：　以带有玻璃涂层的氧化铝微粉、小尺寸板晶(样板晶)和Y-TZP微粉为原料,在常压、不同温度下,通过样板晶生长制备了Y-TZP/板状氧化铝复相陶瓷。对该复相陶瓷的室温力学性能的研究表明,在适当烧结温度下制备的复相陶瓷该材料具有较高的强度(800～900MPa)和断裂韧性(11.8～15.2MPa·m1/2)。用扫描电子显微镜观察复相陶瓷的显微结构特点,表明该材料的增韧机制为氧化锆相变增韧和板晶对裂纹偏转和桥连机制共同起作用。用二参数Weibull分布来量化强度波动,表明该复相陶瓷具有很高的Weibull模量。With alumina platelets and powders coated with 3 wt% CaO-SiO2 glass and yttria-stabilized zirconia (3Y-TZP) powders as raw materials. The compacts were prepared in atmospheric pressure at various temperatures by templated grain growth. The mechanical properties of the composites were investigated. The results show that the composites sintered at proper temperature have high strength (800-900 MPa) and toughness (11.8-15.2 MPa&middotm1/2). The microstructures of the composites were observed using SEM. The possible mechanism could be attributed to the enhancement of phase transformation from tetragonal to monoclinic during fracture and crack-deflection and bridging produced by the platelike A12O3 grains. The variability in strength was quantified by using conventional two-parameter Weibull statistics. The results show that the composite containing higher platelet-alumina has a high Weibull modulus.

关 键 词：样本晶生长 氧化铝板晶 Y-TZP 力学性能 可靠性 

分 类 号：TQ174[化学工程—陶瓷工业] TB332[化学工程—硅酸盐工业]