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作 者:訾振发[1] 王佩红[1] 周圣明[1] 胡国光[1] 尹平[1]
出 处:《磁性材料及器件》2004年第1期20-23,共4页Journal of Magnetic Materials and Devices
摘 要:采用化学共沉法制备了Ni0.6Zn0.4Fe2-xAlxO4(x=0~0.12)纳米粉体,用XRD分析了粉体物相;测量了样品的居里温度TC、起始磁导率i、矫顽力Hc、电阻率ρ、介电损耗角正切tanδe和磁损耗角正切tanδm、摆幅磁感应强度△B。结果表明:样品均为单相的尖晶石结构。Al3+有效地抑制了Fe2+的产生,使NiZn铁氧体的电阻率ρ增大,介电损耗角正切tanδe和磁损耗角正切tanδm下降,Al3+替代Fe3+,居里温度TC和摆幅磁感应强度△B仍保持较高的数值。这种方法是一种提高高频大功率NiZn铁氧体性能的有效方法。Nanosized Ni0.6Zn0.4Fe2-xAlxO4 (x=0 to 0.12 ) powders were prepared by using the chemical co-precipitation method. The phase structure was characterized by X-ray diffraction (XRD). The Curie temperature TC, initial susceptibility i , electrical resistivity ρ, magnetic and dielectric loss tangent (tanδm , tanδe), coercive force Hc , swing flux △B of all samples were measured. The results indicate that all samples are single-phase compounds with spinel structure. With Al3+ substitution for Fe3+, Fe2+ is restrained effectively, making the resistivityρof ferrite increased, tanδm and tanδe decreased. Swing flux density △B becomes large, as well the Curie temperature TC still keep considerably high for Al3+-substituted NiZn ferrites. This is an effective method to improve the properties of NiZn ferrite.
关 键 词:NIZN铁氧体 化学共沉法 居里温度 磁导率 介电损耗和磁损耗
分 类 号:TM277.1[一般工业技术—材料科学与工程]
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