排石饮液质量标准的研究  

Study on quality standards for Paishi Yinye

作　　者：刘凯[1] 王清华[1] 冯丹[1] 

机构地区：[1]黑龙江省药品检验所,黑龙江哈尔滨150001

出　　处：《中国现代应用药学》2004年第1期55-56,共2页Chinese Journal of Modern Applied Pharmacy

摘　　要：目的　建立了排石饮液的质量标准。方法　采用TLC对处方中的虎杖、白芍和丹参进行鉴别 ;用高效液相色谱法测定芍药苷的含量。结果　在TLC色谱中均能检出虎杖、白芍和丹参 ;芍药苷的含量限度不低于 0 .2 6mg/mL。结论　所建立的方法简便可行 ,重现性好 ,提供了排石饮液的质量控制方法。OBJECTIVE To establish the quality standards for Paishi Yinye. METHOD Rhizoma Polygoni Cuspidati,Radix Paeoniae Alba and Radix Salviae Miltiorrhizae in this prescription were identified by TLC. Paeoniflorin was determined by HPLC.RESULTS Rhizoma Polygoni Cuspidati,Radix Paeoniae Alba and Radix Salviae Miltiorrhizae could be detected by TLC. The content limit of Paeoniflorin wasn't lower than 0.26mg/mL.CONCLUSION The established methods are simple, feasible and reproducible. This study provides a method for the quality control of Paishi Yinye.

关 键 词：排石饮液 芍药苷 HPLC 薄层鉴别 

分 类 号：R975.2[医药卫生—药品] R927.2[医药卫生—药学]