“摇头丸”片剂的GC/MS检验  

Determination of rolling pills by GC/MS

作　　者：张春水[1] 刘克林[1] 郑珲[1] 何毅[1] 王朝虹[1] 王炯[1] 

机构地区：[1]公安部物证鉴定中心,北京100038

出　　处：《武汉化工学院学报》2004年第1期9-10,共2页Journal of Wuhan Institute of Chemical Technology

基　　金：国家九五重点科技项目计化子专题部分工作(96-919-01-05-1)

摘　　要：对一例缉获的"摇头丸"片剂毒品进行了GC/MS快速定性、定量检验,检出主要毒品成份为甲基苯丙胺,添加剂有麻黄素、咖啡因、氯胺酮,并对其含量和合成情况进行了分析.工作曲线为C(mg/L)=3.2817×10-6×A+0.01592,相关系数r=0.9972;平均回收率90.3%,标准偏差0.65,变异系数1.3%(n=5);样品含量为7.35%.为分析、推断该类毒品的制作过程提供了一定的借鉴作用.A case of drugs was determined by GC/MS,methamphetamine,ephedrine,caffeine and katemine were found,content and synthetical route were also reviewed,work curve was followed as: C (mg/L)=(3.281 7×10^(-6)× A +0.015 92), r =0.997 2,average recovery was 90.3%,SD was 0.65,C.V. was 1.3%( n =5),content of sample was 7.35%.A method to identify drugs synthesis is provides.

关 键 词：摇头丸 甲基苯丙胺 气相色谱/质谱联用 

分 类 号：O658[理学—分析化学]