醌胺聚合物合成工艺的优化  

Optimization of Synthetic Process of Quinone - Amine Polymer

作　　者：万俊杰[1] 钟宏[1] 

机构地区：[1]中南大学化学化工学院,湖南长沙410083

出　　处：《河南化工》2004年第3期21-22,共2页Henan Chemical Industry

摘　　要：采用溶液聚合法合成醌胺聚合物,运用正交试验设计研究了原料配比、反应时间和温度对反应产率的影响,通过直观分析和方差分析获得了优化的聚合工艺。最佳反应条件为:n(PBQ):n(EDA)=3:1,反应温度20℃,反应时间3h。Quinone - amine polymer is synthesized by solution polymerization. The influences of raw materials formulation and reaction time and temperature on the yield of the reaction is studied by orthogonal experimental design. The optimal polymerization process is obtained by means of visual analysis and variance analysis. The optimal conditions are as follows: the ratio of PBQ to EDA is 3:1; reaction temperature 20℃; reaction time 3h.

关 键 词：醌胺聚合物 正交试验 溶液聚合 合成工艺 工艺优化 

分 类 号：TQ244[化学工程—有机化工]