采用毛细管气相色谱法分析甲基三甲氧基硅烷  

Determination of metheyltrimethoxysilane by capillary chromatography

作　　者：关薇薇[1] 陈江[1] 张荣泉[1] 张翊[1] 

机构地区：[1]蚌埠医学院化学教研室,安徽蚌埠233003

出　　处：《有机硅材料》2004年第1期20-21,共2页Silicone Material

摘　　要：建立了采用毛细管气相色谱仪分析甲基三甲氧基硅烷纯度的方法。该法具有快速、准确、精密度高的优点 ,两种样品 (甲基三甲氧基硅烷的质量分数分别为 70 2 0 %和 93 44% ) 5次平行测定结果的标准误差均为 0 82 ,变异系数分别为 1 1 7%和 0 87%。The method of capillary gas chromatography was used to analyze metheyltrimethoxysilane.It was characterized by rapid,accurate and precise.Two samples which the mass fraction of metheyltrimethoxysilane was 70.20% and 93.44%,the relative standard deviation of 5 parallel measurements was 0.82,and its alteration index was 1.17% and 0.87% respectively.

关 键 词：毛细管气相色谱法 甲基三甲氧基硅烷 纯度 质量分数 变异系数 误差 硅烷交联剂 

分 类 号：TQ264.1[化学工程—有机化工]