肉苁蓉中苯乙醇甙类化合物的LC-MS分析  

Determination of Phenylethanoid Glycosides from Cistanche deserticola in Spring and Autumn with LC-MS

作　　者：曹振杰[1] 赵文军[1] 吴雪萍[1] 

机构地区：[1]中国科学院新疆理化技术研究所,乌鲁木齐830011

出　　处：《中药材》2004年第3期175-177,共3页Journal of Chinese Medicinal Materials

摘　　要：目的 :研究肉苁蓉 (CistanchedeserticolaY C Ma)在不同采收季节苯乙醇甙类化合物含量的变化。方法 :采用LC MS法对肉苁蓉中的四种苯乙醇甙类化合物 (麦角甾甙、海胆甙、肉苁蓉甙A、2′ 乙酰基麦角甾甙 )进行定性分析和含量测定。结果 :在春季和秋季肉苁蓉中分别检测出了四个苯乙醇甙类化合物 ,但除麦角甾甙外 ,其余三种化合物的含量有较大的差别。结论 :肉苁蓉采收季节不同 ,苯乙醇甙类化合物的含量也不同 ,药材质量有一定的差异。Objective:To have a contrast study on phenylethanoid glycosides from Cistanche deserticola Y. C. Ma collected in different seasons.Methods: LC/MS method has been applied for the analysis of four kinds of phenylethanoid glycosides compunds (echinacoside,acteoside,cistanoside A and 2′-acetylacteoside) from Cistanche deserticola Y.C.Ma in spring and autumn.Results:According to the special MS spectra and HPLC chromatogram,this four kinds of phenylethanoid glycosides compounds were detected in each Cistanche deserticola Y.C.Ma,but the content is considerable different except the acteoside.Conclusion:The content of phenylethanoid glycosides from Cistanche deserticola Y.C.Ma in different seasons has a difference from each other,the quality of Cistanche deserticola Y.C.Ma is also different.

关 键 词：肉苁蓉 苯乙醇甙类化合物 LC—MS分析 中药 

分 类 号：R284.1[医药卫生—中药学]