金矿样品的几种溶样方法  被引量:10

Study on several methods of decomposition of ore sample containing gold

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作  者:杨明荣[1] 孙鹏[1] 牟长贤 石爱萍[1] 

机构地区:[1]武警黄金第六支队,河南三门峡472000

出  处:《黄金地质》2004年第1期68-70,共3页Gold Geology

摘  要:通过王水、封闭和烧杯敞口及聚乙烯溶样瓶封闭溶样等方法,对含Au矿样的试样分解、溶样体系及各种溶样方法的对比表明,利用聚乙烯溶样瓶,采用HNO3+NaCl+KMnO4+NH4HF2溶样体系,在水浴锅中封闭溶样40min,矿样中的Au即可完全分解。经国家标准物质分析验证,结果与标准值相符。封闭溶样可以避免样品外溢、迸溅,使分析结果更准确可靠,降低成本,减少环境污染,适用于大批量样品分析。Several methods have been conducted to compare the decomposition methods of samples containing Au,sample-dissolving systems and various sample-dissolving methods by using aqua regia,sealed and open beakers and sealed sample-dissolving in polyethylene sample-dissolving bottle.Using dissolving system HNO_3+NaCl+KMnO_4, Au in samples decomposed completely in water-bathing bottles in less than 40 minutes.Verified by the national standard reference materials,the results are in concord with the standard values.Dissolving samples in sealed bottles can avoid sample-overflowing externally and make the results more accurate and confidence and reduce prime cost;moreover,diminish environmental pollution.It is suitable to analyses in great number of samples.

关 键 词:金矿 试样分解 封闭溶样 标准物质分析 

分 类 号:P617.9[天文地球—矿床学] P618.51[天文地球—地质学]

 

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