微波场协同提取远志皂甙的研究  

Research of Onjisaponins Extraction Assisted with Microwave Field

作　　者：龚盛昭[1] 曾海宇[1] 陈秋基[1] 

机构地区：[1]广东轻工职业技术学院轻化工程系,广州510300

出　　处：《广州食品工业科技》2004年第1期36-38,共3页

摘　　要：以95%乙醇为溶剂,进行了微波场协同提取远志皂甙的研究,得到了微波场协同提取远志皂甙的最佳工艺条件:m(溶剂)/m(远志粉)=18,t=10min,微波功率300W提取2次。将提取液真空浓缩后,用丙酮-乙醚混合液沉析,生成淡黄色沉淀,过滤,沉淀真空干燥,即得远志皂甙粗产品,产率6.34%。与直接加热提取法进行了比较,结果表明微波场协同提取能大大缩短提取时间,并能提高远志皂甙产率。Using 95% ethanol as solvent, onjisaponins was extracted with assistance of microwave field. The optimal technology conditions were obtained as follows. Extract 2 times with assistance of microwave field ( mass ratio of water to material 18:1, time 10min,microwave power 300W). Concentrate the filtrate under vacuum and add the mixture of ether and acetone to deposit. Crude product of onjisaponins is obtained in 6.34% yield after the deposition dried under vacuum. Compared with direct-heating extraction, microwave field-assisted extraction can shorten extracting duration and improve yield of onjisaponins.

关 键 词：微波场协同提取技术 远志皂甙 工艺条件 产率 中药 液料质量比 微波功率 

分 类 号：TQ28[化学工程—有机化工]