对苯二甲醛双缩硫代氨基脲的合成与晶体结构  

Synthesis and Characterization of Terephthaldehyde bis-thiosemicarbazone

作　　者：缪谦[1] 胡茂林[1] 程亚倩[1] 潘启鸿[1] 

机构地区：[1]温州师范学院化学与材料科学学院,温州325027

出　　处：《应用化学》2004年第5期527-529,共3页Chinese Journal of Applied Chemistry

基　　金：浙江省自然科学基金资助项目 (2 0 2 13 7)

摘　　要：A novel Schiff base was synthesized by the reaction of terephthaldehyde with thiosemicarbazide. The structure was confirmed by elemental analysis, IR, UV-vis, 1H NMR and X-ray single crystal diffractometry and the composition of the compound is identified as C16H26N8O2S2. The preliminary anti-bacterial activity tests showed the Schiff base possesses an inhibition activity towards Escherichia Coli, Staphylococcus aureus and Bacillus subtilis.A novel Schiff base was synthesized by the reaction of terephthaldehyde with thiosemicarbazide. The structure was confirmed by elemental analysis, IR, UV-vis, ~1H NMR and X-ray single crystal diffractometry and the composition of the compound is identified as C_16H_26N_8O_2S_2. The preliminary anti-bacterial activity tests showed the Schiff base possesses an inhibition activity towards Escherichia Coli, Staphylococcus aureus and Bacillus subtilis.

关 键 词：对苯二甲醛双缩硫代氨基脲 合成 晶体结构 杀菌活性 

分 类 号：O626.11[理学—有机化学]