Zn(Oxin)_2·2H_2O纳米晶的固相化学反应合成及表征  

Solid State Chemical Reaction Synthesis and Characterization of Nanocrystalline Zn(Oxin)_2·2H_2O

作　　者：李道华[1] 忻新泉[2] 

机构地区：[1]西昌学院,西昌615022 [2]南京大学配位化学研究所,配位化学国家重点实验室,南京210093

出　　处：《无机化学学报》2004年第7期873-878,共6页Chinese Journal of Inorganic Chemistry

基　　金：国家自然科学基金(No.29631040);四川省教育厅自然科学基金(No.2000-B33)资助项目。

摘　　要：Nanocrystalline Zn(Oxin)2·2H2O (Zinc 8-quinolinolate) was synthesized at near ambient temperature by solid state chemical reaction. Phases, particle sizes and morphology of the prepared nanocrystallite were characterized by Powder X-ray diffraction (XRD) and transmission electron microscopy(TEM). The results showed that the crystallite product had an average size about 30 nm. The effects of a series of reaction conditions on the synthesis of Zn(Oxin)2·2H2O (Zinc 8-quinolinolate) by solid state reaction were studied.Nanocrystalline Zn(Oxin)2·2H2O (Zinc 8-quinolinolate) was synthesized at near ambient temperature by solid state chemical reaction. Phases, particle sizes and morphology of the prepared nanocrystallite were characterized by Powder X-ray diffraction (XRD) and transmission electron microscopy(TEM). The results showed that the crystallite product had an average size about 30 nm. The effects of a series of reaction conditions on the synthesis of Zn(Oxin)2·2H2O (Zinc 8-quinolinolate) by solid state reaction were studied.

关 键 词：纳米超细微粒 固相化学反应 合成 8-羟基喹啉锌 纳米材料 

分 类 号：O614.241[理学—无机化学] TB383[理学—化学]