银黄狼消颗粒剂检测方法研究  

Study on qualitative and quantitative methods for Yinhuang Liangxiao granule

作　　者：李先端[1] 仝燕[1] 马振山[1] 王琳[1] 

机构地区：[1]中国中医研究院中药研究所,北京100700

出　　处：《中国中药杂志》2004年第5期426-428,共3页China Journal of Chinese Materia Medica

摘　　要：目的 :建立银黄狼消颗粒质量标准 ;方法 :采用薄层层析定性 ,反相高效液相定量 ;结果 :建立金银花、青蒿、三七、紫草、山茱萸的鉴别方法 ,大黄中大黄酚的含量测定法。结论 :经方法学考察和 3批样品验证 ,方法准确 ,简便灵敏 ,可作为本制剂质量标准 ,并供其他复方制剂的参考。Objective: To establish the quality standard of Yinhuang Langxiao granule. Method: The Panax notoginseng, Arnebia euchromq,Cornus officinalis,Lonicera japonica,Artemisiae annua were identified by TLC. The content of chrysophanol in granule was determined by HPLC. Result: Spots of samples on TLC can be well separated and the method had good specificity. The average recovery of chrysophanol was 98.7% and RSD was 0.67%. Conclusion: An acurate,simple and effective quality-controlling method has been developed, which can be used for quality control for Yinhuang Langxiao granule.

关 键 词：银黄狼消颗粒剂 检测方法 金银花薄层 青蒿薄层 高效液相法 

分 类 号：R286[医药卫生—中药学]