蜂蜜中氯霉素残留量的色谱分析  

Chromatography Analysis of Chloromycetin Residual Quantity in Honey

作　　者：胡大晰 李庆才[1] 

机构地区：[1]烟台师范学院化学系,吉林进出口商品检验局

出　　处：《烟台师范学院学报（自然科学版）》1994年第2期121-124,共4页Yantai Teachers University journal(Natural Science Edition)

摘　　要：应用高效液相色谱法定量分析出口蜂蜜中氯霉素残留量。样品用去离子水溶解后，经１－ｘ_８吸附树脂柱净化和富集，在ＷａｔｅｒｓＣ_（１８）柱上分离，紫外测定，检测下限为０．０１μｇ／ｇ，回收率为８６．３７％～１０１．５％，相对标准偏差为５．８６％～１１．９２％。Quantitative analysis of chloromycetin residual quantity in export honey has been taken by efficient liquid chromatography.Sample dissolved into non-ion water has been pured and richened by 1-x_8 adsorption reisen column,and seperated by Water C18 column.UV determination,low limit of examination is 0.01μg/g, rate of recovery is 86.37%～101.5%,relative standard deviation is 5.86%～11.92%.

关 键 词：高效液相色谱 蜂蜜 氯霉素 残留量 

分 类 号：S894.1[农业科学—特种经济动物饲养]