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出 处:《中国实验方剂学杂志》2006年第1期15-17,共3页Chinese Journal of Experimental Traditional Medical Formulae
摘 要:确定肤痒茶剂质量标准。通过薄层鉴别方法对处方中地肤子、苍耳子、红花进行定性鉴别。运用高效液相色谱法对川芎中的阿魏酸进行含量测定。定性鉴别能从样品中检出相应的斑点。含量测定阿魏酸量在0.0222-0.1110Mg有良好的线性关系,回收率101.02%,RSD=1.81%。所建立的方法可靠,能准确地进行定性、定量检测,可用于该制剂的质量控制。To establish the quality standard for Fuyang tea. Kochia scoparia (L.)Schrad., Xanthium sibiricum Patr. and Carthamus tinctorius L. were identified by TLC. Ferulic Acid was determined by an HPLC method:A good linear relationship between peak area and concentration of ferulic acid was found at the range of 0.0222 - 0. lll0ttg with a correlation coefficient of A = 0.9993.The average recovery of ferulic acid was 101.02% and RSD was 1.81% (n = 5). The method is reliable, accurate and specific. It can be used for the quality control of Fuyang tea.
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