丁香油β-环糊精包合前后化学成分的GC-MS分析  

GC-MS Analysis of Chemical Components of Clove Oil before and after β-cyclodextrin Inclusion

作　　者：夏春秀[1] 李宗[2] 

机构地区：[1]福建中医学院药学系,福州350003 [2]福建省药品检验所,福州350001

出　　处：《中药新药与临床药理》2006年第3期214-215,共2页Traditional Chinese Drug Research and Clinical Pharmacology

摘　　要：目的对β-环糊精包合前后的丁香油组分进行分析。方法采用GC-MS法对化学成分进行分离鉴定。DB-1毛细管气相色谱柱,程序升温:60℃(1min)10℃/min230℃(3min);分流进样,分流比:1∶50;进样口温度:230℃,MS检测。结果经GC-MS分析,包合前后丁香油主要成分基本一致,但各组成比例发生变化。结论β-环糊精对化合物的包合会使丁香油化学成分的比例在包合前后发生一定的变化。Objective To analyze the chemical components of clove oil before and after β- cyclodextrin inclusion. Methods GC - MS conditions were as follows： DB - 1 Capillary gas chromatographic column, programmed temperature rising from 60 ℃ to 230 ℃ at the rate of 10 ℃/min; split ratio being 1 ： 50, Injector port temperature at 230 ℃ and Flame Ionization Detec- tor（FID） temperature at 230 ℃. The components were detected by MS detector. Results GC - MS analysis showed that the main components of clove oil did not changed before and after inclusion, but the proportion of the components had been changed. Conclusion β- cyclodextrin inclusion have effects on the proportion of clove oil components.

关 键 词：丁香油 Β-环糊精 化学成分 GC-MS分析 

分 类 号：R284.1[医药卫生—中药学]