N,N-二烯丙基-5-甲氧基色胺的合成研究  

Study on the synthesis of N,N-diallyl-5-methoxytryptamine

作　　者：赵宏伟[1] 洪镛裕[1] 刘超程[1] 

机构地区：[1]华东师范大学化学系,上海200062

出　　处：《化学试剂》2006年第5期307-308,共2页Chemical Reagents

摘　　要：以5-甲氧基吲哚为原料,依次经过Vilsmeierβ-甲酰化、加成、还原,最后在碘化钾催化下和烯丙基氯发生取代反应,简捷、高效地合成了N,N-二烯丙基-5-甲氧基色胺。其结构经红外光谱、质谱、核磁氢谱分析确证。N, N-diallyl-5-methoxytryptamine was synthesized with 5-methoxyindole as raw materials via a series of Vilsmeier formylation, addition, reductive and substitution at the catalysis of KI with allyl chloride. The product was characterized by IR, GCMS and ^1HNMR.

关 键 词：5-甲氧基吲哚 Vilsmeier β-甲酰化 N N-二烯丙基-5-甲氧基色胺 

分 类 号：O626[理学—有机化学]