2-叔丁氨基-4-环丙氨基-6-甲巯基-S-三嗪的制备  

The synthesis of 2-(tert-butylamino)-4-(cyclopropylamino)-6-(methylthio)-S-triazine

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作  者:宋静[1] 洪镛裕[1] 刘超程[1] 

机构地区:[1]华东师范大学化学系,上海200062

出  处:《化学试剂》2006年第8期505-506,共2页Chemical Reagents

摘  要:以氰尿酰氯为原料,分别用环丙胺、叔丁胺、硫醇钠经过3次取代得到高纯度的目标化合物,收率90%。2-( tert-Butylamino )-4-( cyclopropylamino )-6- (methylthio)-S-triazin was-prepared by successive three-step adclition processes to cyanufic chloride. In subsequent treatment, the product was precipitated by changing the polarity of the reagents. The synthesis was suitable for industry with its product being stable, its preparation being easily carried out and solvents being readily recovered with high percentage.

关 键 词:氰尿酰氯 环丙胺 叔丁胺 硫醇钠 

分 类 号:O626[理学—有机化学]

 

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