超声波强化有机溶剂提取万寿菊中叶黄素的研究  

Study on Ultrasonic-assisted Solvent Extraction of Lutein from Tagetes eracta Linn.

作　　者：李大婧[1] 方桂珍[2] 刘春泉[3] 

机构地区：[1]东北林业大学林学院,黑龙江哈尔滨150040 [2]东北林业大学材料科学与工程学院,黑龙江哈尔滨150040 [3]江苏省农科院原子能农业利用研究所,江苏南京210014

出　　处：《林产化学与工业》2006年第3期127-130,共4页Chemistry and Industry of Forest Products

基　　金：江苏省农业科学院科研基金资助项目(6110537)

摘　　要：研究超声波强化有机溶剂提取万寿菊花粉中叶黄素的工艺过程,考察了萃取率的影响因素。结果表明,正己烷和石油醚作提取溶剂效果较好。以1.000 g万寿菊花粉为原料,超声波强化正己烷的较优提取条件为:料液比1∶20(g∶mL,以下同),超声波功率300 W,超声波作用时间30 m in,叶黄素提取率93.65%;强化石油醚的较优条件为:料液比1∶20,超声波功率400 W,超声波作用时间30 m in,叶黄素提取率98.77%。The use of ultrasonic-assisted solvent extraction of lutein from flower of marigold （ Tagetes erecta Linn. ） under different operating conditions was studied. Influences of solvent, ratio of material to liquid, ultrasonic power and ultrasonic treatment time on the extraction yield of lutein were studied. It was found that both n-hexane and petroleum ether were good solvent for ultrasonic-assisted process. Optimal ultrasonic-assisted n-hexane and petroleum ether extraction conditions for 1. 000 g marigold flower powder were： 1：20（g： mL） for ratio of material to liquid, 30 min for ultrasonic time, 300 W and 400 W for ultrasonic power, and extraction rates were 93.65 % and 98.77 %, respectively.

关 键 词：叶黄素 超声波辅助提取 万寿菊 

分 类 号：TQ91[化学工程] Q562[生物学—生物化学]