乙撑双硬脂酰胺的制备  

A novel synthesis of ethylene bis stearamide

作　　者：张颖[1] 谢斌[2] 田桂芝[1] 王茹[1] 

机构地区：[1]抚顺职业技术学院,辽宁抚顺113006 [2]中国石油吉林石化公司,吉林吉林132021

出　　处：《化工科技》2006年第5期1-3,共3页Science & Technology in Chemical Industry

基　　金：国家重点新产品计划项目(2002ED650028)

摘　　要：以乙二胺和硬脂酸为原料制备乙撑双硬脂酰胺,考查了原料配比、滴加时间、反应温度对产品收率的影响,确定合成工艺的最佳条件为:硬脂酸与乙二胺的摩尔比2.5∶1,滴加时间1 h,反应温度160℃,最高收率98.12%。产物结构用红外光谱、元素分析等方法进行表征。Preparation of ethylene his stearamide using stearic acid and ethylenediamine as raw materials has been studied. The effect of the molar ratio of raw material,titration time, reaction temperature on the of the product are observed. Optimum conditions of synthesizing technology were deterra ethylenediamine= 2.5 ： 1, titration time was 1 hours, reaction temperature was 160 ℃. The yield of the product reached 98.12 %. Structure of objective product was characterized by IR and elementary analysis.

关 键 词：乙撑双硬脂酰胺 乙二胺 硬脂酸 

分 类 号：TQ225.261[化学工程—有机化工]