微波辐射下8-溴腺苷及其衍生物的绿色合成  

Green Synthesis of 8-Bromoadenosine and Its Derivatives under Microwave Irradiation

作　　者：渠桂荣[1] 张志广[1] 郭海明[1] 夏然[1] 耿明伟[1] 

机构地区：[1]河南师范大学化学与环境科学学院,河南新乡453007

出　　处：《合成化学》2007年第2期195-197,共3页Chinese Journal of Synthetic Chemistry

基　　金：国家自然科学基金资助项目(20372018)

摘　　要：以Br2为溴化试剂，水为溶剂，微波辐射5min，合成了6种8-溴腺苷衍生物，收率76％-85％，其结构经^1HNMR，HR-MS和元素分析表征。Using Br2 as a bromination reagent and water as a solvent, 8-bromoadenosine and its six derivatives were obtained in 76% -85% yields under microwave irradiation for 5 min. The structures were confirmed by ^1H NMR, HR-MS and MS.

关 键 词：腺苷 溴化 绿色溶剂 微波辐射 绿色合成 

分 类 号：O621.25[理学—有机化学]