两种口腔镍铬合金离子析出的体外实验研究  

Effects of salivary contents and pH on element released from Ni-Cr dental alloys

作　　者：杨敏[1] 陈树国[2] 孟令强[2] 张钊[2] 沈文静[2] 

机构地区：[1]天津市口腔医院,300041 [2]河北医科大学口腔医学院

出　　处：《现代口腔医学杂志》2007年第3期300-303,共4页Journal of Modern Stomatology

基　　金：河北省科技厅资助项目(03276196D-46)

摘　　要：目的研究HeraeniumS与TILITE P两种口腔镍铬合金在唾液pH值和成分变化时离子析出行为。方法将两种合金试件在pH6.8正常唾液环境中浸泡一周,再用pH4的酸性及酸性加0.1%F-的人工唾液处理两小时,之后回到正常唾液环境中浸泡一周,观察其在处理前、后镍离子的析出和表面理化状态的改变。结果①在正常唾液环境中HeraeniumS合金镍离子的析出量大于TILITE P合金;②pH降低和氟化物的加入增大了两种合金镍离子的析出量,其中TILITE P合金大于HeraeniumS合金;③在短暂的pH降低和加入氟化物后再回到正常唾液环境中,TILITE P合金的镍离子析出量大于HeraeniumS合金;并且在合金表面可以观察到形态学上的腐蚀破坏。结论口腔镍铬合金的镍离子析出受到口腔环境动态变化的影响,TILITE P合金对环境改变的敏感性更大。Objective To examine the effects of salivary contents and pH on elements released from Ni - Cr dental alloy Heraenium S and TILITE P in different pH and contents of saliva. Methods Eighteen specimens for each alloy were first immersed in pH 6,8 AS （represented the normal salivary environment in oral cavity） for one week. Then the specimens were treated with pH 4 AS and pH 4 AS containing 0.1% F- for two hours, respectively. The release of nickel ion was measured after the treatments with atomic absorption spectrophotometry, Changes of alloy surface were also observed with scanning electron microscope and X - ray photoelectron spectroscopy. Results The release of nickel ion from Heraenium S was higher than that from TILITE P in normal salivary environment. The release of nickel ion from both alloys was higher in saliva with lower pH and the presence of fluoride than in normal salivary environment. In saliva with lower pH and the presence of fluoride, the release of nickel ion from TILITE P was higher than from Heraenium S. After transient treated with lower pH and the presence of fluoride, the release of nickel ion from TILITE P became higher than that from Heraenium S in the normal saliva environment, and corrosion on the surface of TILITE P was also observed. Conclusion The release of nickel ion from Ni- Cr dental alloys may be affected by the dynamic oral environment and TILITE P appears to be more sensitive to environmental changes.

关 键 词：口腔铸造合金 镍铬合金 离子析出 腐蚀 

分 类 号：R783.1[医药卫生—口腔医学]