微波条件下季戊四醇双磷酰氯的合成  

Synthesis of Pentaerythritol Phosphonyl Dichloride by Microwave Radiation

作　　者：张鄞[1] 

机构地区：[1]云南省化工研究院,云南昆明650041

出　　处：《云南化工》2007年第4期17-20,共4页Yunnan Chemical Technology

摘　　要：以季戊四醇和三氯氧磷为原料,在微波条件下合成季戊四醇双磷酰氯,此方法与其他方法相比显著降低了反应温度,加快了反应速度,提高了反应收率。分析结果确证反应产物为目标产物。　Pentaerythritol phosphonyl dichloride was prepared from phosphoryl chloride and pentaerythritol by microwave irradiation.Result showed that reaction temperature and time were reduced and structure of the product was supported by analytical date.

关 键 词：微波条件 季戊四醇双磷酰氯 合成 

分 类 号：TQ314.248[化学工程—高聚物工业]