八角茴香油臭氧化制备茴香醛工艺研究  

Preparation of Anisaldehyde from Star Anise Oil by Ozonolysis Reaction

作　　者：高蓉[1] 李稳宏[1] 李冬[1] 韦玮[2] 郭楠[1] 赵鹏[1] 

机构地区：[1]西北大学化工学院,陕西西安710069 [2]复旦大学光科学与工程系,上海200433

出　　处：《食品科学》2008年第6期174-177,共4页Food Science

摘　　要：以八角茴香油为原料,采用臭氧氧化法制备茴香醛。在单因素试验和Box-Benhnken试验设计基础上,进行试验及回归分析得到最佳工艺参数:氧化反应时间21min,氧化温度8.45℃,复合溶剂配比4.27:1(g/g),收率可达73.6%。验证实验显示,最优条件下实验结果能够很好地与预测值符合。The preparation of anisaldehyde by ozonolysis reaction from star anise oil was studied. The single-factor extraction tests and Box-Behnken design were employed to determine the optimum technological condition. The optimal experiment parameters are： reaction time 21 min, reaction temperature 8.45℃, two solvents ratio 4.27：1 （g/g）. Confirmatory experiment results showed that the yield is up to 73.6% under above-mentioned conditions.

关 键 词：八角茴香油 茴香脑 茴香醛 臭氧氧化 响应面分析 

分 类 号：TQ041[化学工程]