双(α-呋喃丙烯酸)氧钒配合物的合成  

Synthesis of Bis(α-Furylacrylic Acid) Oxovanadium Complex

作　　者：李俊海[1] 孙纲春[1] 

机构地区：[1]河南工业大学化学化工学院,河南郑州450001

出　　处：《化学与生物工程》2008年第8期10-11,共2页Chemistry & Bioengineering

基　　金：河南工业大学引进人才资助项目(150207)

摘　　要：采用两种方法合成了α-呋喃丙烯酸与有机钒配合物双(α-呋喃丙烯酸)氧钒,并对该配合物的合成方法进行了改进,对其结构进行了表征。方法一:由VOSO4和α-呋喃丙烯酸在水溶液中直接反应制得;方法二:由VOSO4和α-呋喃丙烯酸钡发生沉淀反应制得。结果表明,方法一的产率更高。α-Furylacrylic acid and bis（α-furylacrylic alid） oxovanadium complex were designed and synthe-sized. The synthesis of bis（α-furylacrylic acid） oxovanadium complex was improved and explored with two methods. In aqueous solution, this compound was synthesized with VOSO4 and a-furylacrylic acid directly by the first method; this compound was synthesized with VOSO4 and α-furylacrylic acid barium by the second method. The yield of the first method was higher.

关 键 词：Α-呋喃丙烯酸 氧钒配合物 合成 

分 类 号：TQ251.1[化学工程—有机化工] R965.1[医药卫生—药理学]